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In the binary system, the initiating radical is generated by the RT mechanism via thermolysis of the carbon-tellurium (C-Te) bond in a dormant species, and this process is the rate-determining step. Once the radical is generated, the polymerization proceeds mainly by the DT mechanism. In contrast, as the initiating radical is provided from azo-initiators under mild thermal conditions in the ternary system, the polymerization exclusively proceeds by the DT mechanism.

Since 2 is an excellent CTA,32,67–69 it undergoes DT-mediated polymerization, affording 4. The other proceeds via the initial addition of 7 to the monomer, eventually affording 4 by DT-mediated polymerization. This mechanism indicates that the amount of 4 is proportional to the influx of radical 7 during the polymerization period, and the experimental results are consistent with this mechanism.

However, no apparent rate retardation was observed. Furthermore, the low-temperature polymerization also enhanced the dispersity control. Effect of photoirradiation on the progress of the polymerization of BA in the presence of 1b. Effect of polymerization conditions on the precision synthesis of block copolymers. The formation of 4 is an indication of the formation of dead polymers, and the MS results are consistent with the SEC data.

Routine analyses using size exclusion chromatography were also carried out. Schematic representation of the effect of the radical initiator on polymer-end structures. Measuring Ions A beam of charged particles will ionize gas. –Particle energy E –Chamber area A An applied field will cause ions and electrons.

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; QUEST operation, K.H., H.I., T.O., T.I., K.N., R.I., Y.N., M.H. All authors have read and agreed to the published version of the manuscript. Finally, as a measure of the effect of atoms on the plasma, we evaluated the degree of ionization .